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Read or Download New Types of Persistent Halogenated Compounds (Handbook of Environmental Chemistry, Volume 3 Anthropogenic Compounds, Part K) PDF
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Extra info for New Types of Persistent Halogenated Compounds (Handbook of Environmental Chemistry, Volume 3 Anthropogenic Compounds, Part K)
17, 21] used gel permeation chromatography (GPC) to separate the PCTs from the lipids and also from the PCBs. It was found that the PCTs eluted before most PCBs both on an S-X3 and S-X8 Bio beads column (100 g, 48 J. de Boer 200–400 mesh). The use of dichloromethane as the sole solvent was preferred. S-X3 was considered to give a better separation between PCTs and lipids than S-X8. Onuska et al.  tested microbore and open tubular capillary columns in supercritical fluid chromatography (SFC).
3 Extraction and Clean-Up . . . . . . . . . . . . 47 Gas Chromatography . . . . . . . . . . . . . 48 Mass Spectrometry . . . . . . . . . . . . . . 49 5 Environmental Distribution . . . . . . . . . . . 1 Correlation of PCT and PCB Concentrations . . . . . . . 55 6 Toxicity . . . . . . . . . . . . . . . . . 57 References . . . . . . . . . . . . . . . . . . 58 The Handbook of Environmental Chemistry Vol.
3). As is to be expected, the most prominent peaks in the ECNI spectra are due to the molecular ions. De Boer et al.  have compared the sensitivity of the three detection techniques for TCPM and TCPMe (Table 1). Generally, compounds with less than four chlorine atoms are rather difficult to determine in environmental samples by means of GC/ECNI-MS because of too low a sensitivity . However, for TCPM the electronegativity of the oxygen apparently helps to increase sensitivity and thus to create good analyte detectability for this compound.